RESEARCH IN SYNTHESIS AND CHARACTERIZATION OF HIGHLY ARYLATED ORGANOSILICON COMPOUNDS.
Abstract
A series of six organomonofluorosilanes was prepared via the corresponding chlorosilane analogs by derivatization of the appropriate chlorosilane intermediates with 1-naphthyllithium followed by rehalogenation with a suitable inorganic fluoride. Aqueous hydrofluoric acid (10%) was used in all but the single case of an Si-H-containing compound for which a hexafluorosilicic acid reagent was found to be satisfactory. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Jul 01, 1967
- Accession Number
- AD0663240
Entities
People
- D. C. Smith
- G. M. Hart
- J. W. Ezell
- K. C. Pande
- S. R. Gudemoos