IMPROVED II-VI CRYSTALS.

Abstract

The results of the outgassing study CdS powder shows that most of the gases evolved during vacuum sintering are due to the presence of about 0.1 mole % hydrated CdSO4. It was found that a reduced amount of SiO2 inclusions results if epitaxial crystal growth of CdS is carried out in an unsealed tube under 1 atm Ar. X-ray fluorescence measurements show that CdSe crystals grown in this laboratory contain about 2 mole % S, which can be reduced by a Se-vapor treatment. Analysis of the solid-vapor equilibria for CdS-CdSe mixed crystals shows a variation of Kp with composition, with a pronounced minimum at 0.57 mole fraction CdS. Of extreme importance in determining the electrical properties of II-VI semiconductors are native point defects. A theoretical analysis of their equilibria shows a complex interdependence of the various defects and a necessity for experimentally determining the various equilibrium constants. A verification of the dependence of acoustic amplification properties on S pressure was made, with optimum current oscillations occurring when a minimal S pressure of about 0.2 atm at 850C is used. (Author)

Document Details

Document Type
Technical Report
Publication Date
Mar 06, 1966
Accession Number
AD0666402

Entities

People

  • J. M. Jost
  • L. R. Shiozawa

Tags

DTIC Thesaurus Topics

  • Amplification
  • Buildings And Structures
  • Compound Semiconductors
  • Crystal Growth
  • Crystals
  • Electrical Properties
  • Electronics
  • Fluorescence
  • Inclusions
  • Measurement
  • Oscillation
  • Outgassing
  • Point Defects
  • Research Facilities
  • Semiconductors
  • Sintering
  • X Rays

Fields of Study

  • Materials science

Readers

  • Combustion science or combustion engineering.
  • Materials Science and Engineering.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene