MASS THERMAL ANALYSIS OF HYDROXYLAMINE AND METHOXYAMINE PERCHLORATES

Abstract

Mass thermal analysis was used to study the thermal decomposition of hydroxylamine and methoxyamine perchlorates. The first step in the thermal decomposition of these salts is the proton transfer from the substituted ammonium ion to the perchlorate anion to form the free substituted amine and perchloric acid. Activation energies were determined to be 20.7 kcal/mole (65 to 77C) for the dissociation of hydroxylamine perchlorate, and 30 kcal/mole (53 to 77C) for the dissociation of methoxyamine perchlorate.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1969
Accession Number
AD0692492

Entities

People

  • Berge B. Goshgarian

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Acids
  • Air Force
  • Amines
  • Arrhenius Equation
  • Chlorine Compounds
  • Decomposition
  • Differential Thermal Analysis
  • Dissociation
  • Heat Of Activation
  • Measurement
  • Melting Point
  • Oxidation
  • Perchlorates
  • Perchloric Acid
  • Phase
  • Phase Transformations
  • Thermal Analysis

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry
  • Combustion science or combustion engineering.