SPECTRAL METHOD OF DETERMINING IRON IN FERROCENE AND ITS DERIVATIVES,
Abstract
A spectral method of determining iron in ferrocene and its derivatives is highlighted by speed, high sensitivity and sufficient accuracy. The method consists of mixing a sample and various organic solvents in a retort, then pouring it in a cooling cup fulgurator using a revolving electrode. A low capacity spark was produced. Spectra were then recorded. Most suitable solvents in this procedure are cyclohexanone and kerosene. Probable error for an individual determination is 3.4%. By using silicon as an element of comparison, the feasibility of simultaneous determinations is shown. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Oct 08, 1969
- Accession Number
- AD0700343
Entities
People
- E. A. Kuchkarev
Organizations
- National Air and Space Intelligence Center