THE NATURE OF NON-STOICHIOMETRIC SOLIDS: STRUCTURE, TEXTURE, THERMODYNAMIC AND MAGNETIC PROPERTIES.

Abstract

Experimental studies were carried out on the understanding of non-stoichiometry and disorder in inorganic ionic crystals. A mechanistic model for generating crystollographic shear (CS) structures is proposed. Electron diffraction/microscopy is used for examining the crystals of the various oxides of the outer transition metals. Isobaric studies of the oxides of praeseodymium, curium, and americium are undertaken. Crystallographic shear studies were made on the niobium dioxyfluoride, vanadium oxide and rutile structures. Related thermodynamic measurements are being made with a solid state galvanic cell. Magnetic susceptibility studies have been made on various rare earth oxide systems, including lanthumum, cerium, gadolinium, praeseodymium, titanium, molybdenum, thulium, and ytterbium. Structures of high- and low-temperature forms of the phase of tri-zirconoum tetra-ytterbium duodica oxide have been determined by single x-ray studies. (Author)

Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1970
Accession Number
AD0702473

Entities

People

  • B. G. Hyde
  • B. N. Figgis
  • D. J. M. Bevan

Organizations

  • University of Western Australia

Tags

DTIC Thesaurus Topics

  • Crystals
  • Diffraction
  • Electrochemical Cells
  • Electron Diffraction
  • Ionic Crystals
  • Low Temperature
  • Magnetic Properties
  • Metals
  • Molybdenum
  • Titanium
  • Transition Metals
  • Vanadium
  • X Rays
  • Ytterbium

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Materials Science and Engineering.
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene