A Study of the Radiation Stability and Means of Fabricating MRC Copolymer 250B Films for Dosimeters.

Abstract

The two major objectives of this study were: to identify the factor or factors responsible for the unique radiation stability of MRC Copolymer 250B and to explore various methods for forming dosimeter quality films from polymer powder. Solution casting, blow extrusion, T-die extrusion, and biaxial orientation were studied. All evidence strongly indicates that the sulfate end group resulting from persulfate initiation is the structural feature responsible for radiation stability of MRC Copolymer 250B. There is evidence suggesting that some specific polar end groups are sufficient to impart radiation stability since hydrogen peroxide initiated polymer is also radiation stable. The possibility that a sulfur-containing emulsifier can contribute to radiation stability also exists. With the exception of the persulfate initiation, it was shown that no component of the polymerization recipe contributes to radiation stability. However, since it is necessary to use polymer made by the emulsion technique, the process is important. (Author)

Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1970
Accession Number
AD0715417

Entities

People

  • Earl V. Kirkland
  • George L. Ball Iii
  • Ival O. Salyer
  • Philip H. Wilken
  • Roger L. Seelig

Organizations

  • Monsanto

Tags

DTIC Thesaurus Topics

  • Copolymers
  • Dosimeters
  • Emulsions
  • Extrusion
  • Hydrogen
  • Materials
  • Materials Processing
  • Orientation (Direction)
  • Peroxides
  • Polymerization
  • Polymers
  • Radiation
  • Rocket Oxidizers

Fields of Study

  • Physics

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Nuclear and Radiation Engineering.
  • Polymer Science and Engineering.

Technology Areas

  • Microelectronics