Epoxy Curing Agents. I. Imidazoles,

Abstract

2-Ethyl-4-methylimidazole (EMI-24) cures epoxy adhesives at a moderate temperature and imparts high heat resistance to the product. Due to the tendency of EMI-24 to crystallize at room temperature, this study was undertaken to find a suitable replacement. Resins cured with EMI-24, 1-methylimidazole (MI-1), and imidazole were compared with respect to bond strength and heat deflection temperature as functions of curing-agent concentration and cure conditions. Results indicate that the physical properties of resins cured with MI-1 and imidazole are comparable with that cured with EMI-24. MI-1 has the advantages of being readily available and of being a liquid at room temperature. A published article on the mechanism of imidazole-cured epoxy resins suggests that the pot life of the adhesive system may be increased by placing deactivating substituents on the imidazole ring. Results of a study of such systems are presented. (Author)

Document Details

Document Type
Technical Report
Publication Date
Sep 01, 1971
Accession Number
AD0732345

Entities

People

  • Thomas J. Dearlove

Organizations

  • Harry Diamond Laboratories

Tags

DTIC Thesaurus Topics

  • Adhesives
  • Chemical Reactions
  • Curing
  • Curing Agents
  • Deflection
  • Epoxy Resins
  • Imidazoles
  • Physical Properties
  • Resins
  • Resistance
  • Surface Properties
  • Thermal Properties

Fields of Study

  • Materials science

Readers

  • Organic Chemistry
  • Polymer Science and Engineering.