Studies of the Preparation, Properties and Physicochemical Characterization of Hydroxyethyl Starch for Use as a Volume-Extender for Blood Plasma.

Abstract

The research described is devoted to a study of the physical chemistry and biochemistry of hydroxyethyl starch, and the manner in which these factors are influenced by the molecular architecture of the derivatized polysaccharide. Part of the report contains a detailed literature review of hydroxyethyl starch and the analytical techniques employed for its examination. The authors have differentiated between two terms which are often used interchangeably when describing the hydroxyethyl derivative namely molar substitution (the number of moles of ethylene oxide which react per mole of monomer unit) and degree of substitution (the mole fraction of anhydroglucose units which carry substituent groups). They have developed a technique whereby the content of unsubstituted glucose residues may be rapidly obtained, and thus the determination of the degree of substitution is, for the first time, a relatively simple procedure. The in vitro degradation of the hydroxyethyl derivative by alpha-amylase was also studied. On the basis of these studies, a mathematical model was constructed for the substitution pattern in hydroxyethyl starch which successfully predicts the seeming anomaly of materials of molar substitution greater than unity being hydrolysed by alpha-amylase.

Document Details

Document Type
Technical Report
Publication Date
Aug 31, 1971
Accession Number
AD0732785

Entities

People

  • C. T. Greenwood

Organizations

  • University of Edinburgh

Tags

DTIC Thesaurus Topics

  • Alkenes
  • Biochemistry
  • Blood
  • Blood Plasma
  • Chemical Compounds
  • Chemical Synthesis
  • Chemistry
  • Ethylene Oxide
  • Ethylenes
  • Films
  • Literature Surveys
  • Materials
  • Mathematical Models
  • Organic Chemistry
  • Physical Chemistry

Fields of Study

  • Chemistry

Readers

  • Aquatic Ecology
  • Computational Modeling and Simulation
  • Polymer Science and Technology