Rubber Research: The Synthesis of Unsaturated Fluorocarbons
Abstract
The report describes the synthesis of CF2Cl-CF2NO using NOCl and FeCl3 as a catalyst. The FeCl3 also forms an addition complex with the nitorso compound. The compound, UO2(NO3)2:H2O:N2O4, was used to nitrate CF2=CFCl as a means of producing nitroso compounds by stopping the reaction before completion. The reduction of fluoronitro alkanes was also tried. As a precursor to imine synthesis, CF3-CF2-CF2-CHOH-CH2NO2 was prepared.
Document Details
- Document Type
- Technical Report
- Publication Date
- Dec 10, 1960
- Accession Number
- AD0742484
Entities
People
- J. D. Park
- J. R. Lacher
Organizations
- University of Colorado Boulder