Method of Obtaining Polyfluoroalkyl Dichlorophosphates,
Abstract
A method is reported for obtaining polyfluoroalkyl dichlorophosphates by reacting a polyfluoroalkyl alcohol with phosphorus oxychloride with heating. For simplification of the process, the reaction is conducted in the presence of metal chlorides of the I, II or III group of the periodical system. Phosphorus oxychloride and polyfluoroalkyl alcohol are taken in a ratio of 5 to 1 and the process is conducted at 70-120C. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Mar 20, 1972
- Accession Number
- AD0745447
Entities
People
- L. S. Zakharov
- M. I. Kabachnik
- N. N. Godovikov
- V. V. Pisarenko
Organizations
- National Air and Space Intelligence Center