THM Growth of Materials for Electro-Optic Light Modulators
Abstract
The report summarizes the year's work in growth of crystals of electrooptic materials from a solvent zone (a growth method designated THM). Single crystals of proustite (Ag3AsS3) and a crystal of Bi(12)TiO(20) were achieved. Extensive effort on growth of CdSnAs2 from Sn and CdGeAs2 from Pb zones did not yield useful-sized crystals even after significant improvements in the THM arrangement. Investigations of the phase equilibria determined that in each case a phase other than the desired ternary arsenide was on the verge of crystallizing from the solvent zone. Also, it was deduced that constitutional supercooling occurred in the diffusion boundary layer of the THM runs on both systems. The contrasting results on proustite and the II-IV-V2 compounds are attributed to different degrees of supercooling due to differences of molecular association in the liquid phase.
Document Details
- Document Type
- Technical Report
- Publication Date
- Sep 01, 1972
- Accession Number
- AD0750941
Entities
People
- Andrew A. Menna
- Fritz V. Wald
- John C. Swartz