Analysis of Soluble Beryllium by Gas Chromatography

Abstract

A new microanalytical method for the detection and quantitation of beryllium in aqueous samples and biological specimens has been developed. The method, based upon quantitation of chelated beryllium by gas chromatography, was employed to detect beryllium in both in vitro samples and tissues of rats given beryllium by injection. Beryllium was administered in the form of aqueous solutions of beryllium sulfate, and as little as 10 nanograms beryllium per gram of whole blood were detected and quantitated. In vivo studies which compared gas chromatographic analyses with radiometric analyses confirmed the validity of the new microanalytical technique. Preliminary studies were conducted to determine the ability of fluorinated chelating agents to remove beryllium oxide from the lungs of rats.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1972
Accession Number
AD0753112

Entities

People

  • Eugene L. Arnold
  • Michael L. Taylor

Organizations

  • Monsanto

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Air Force
  • Air Force Facilities
  • Aqueous Solutions
  • Biomedical Research
  • Chelate Compounds
  • Chemistry
  • Chromatographs
  • Chromatography
  • Contracts
  • Detectors
  • Gas Chromatography
  • Hydroxides
  • Hygiene
  • Materials
  • Metals
  • Public Health
  • Water

Readers

  • Analytical Chemistry
  • Rocket Propulsion.
  • Toxicology/Environmental Toxicology