Vacuum Sublimation of Ammonium Perchlorate.

Abstract

Time-of-flight measurements have been made on the flux of molecules from the surface of ammonium salts vaporizing into vacuum. As expected with ammonium halides and ammonium bi-sulfate the TOF distributions correspond to equimolar fluxes of ammonia and the corresponding acid. In the case of ammonium perchlorate the vapor subliming from a single crystal comprised ammonia and perchloric acid. When the source was compressed powder, the vapor was a mixture of lower molecular weight species. This result seems best explained in terms of subsurface decomposition. (Author)

Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1972
Accession Number
AD0753219

Entities

People

  • John B. Fenn
  • Steve Tang

Organizations

  • Purdue University

Tags

DTIC Thesaurus Topics

  • Acids
  • Ammonium Perchlorate
  • Chemical Compounds
  • Cooperation
  • Crystals
  • Decomposition
  • Measurement
  • Molecular Weight
  • Molecules
  • Perchlorates
  • Perchloric Acid
  • Single Crystals
  • Sublimation
  • Vapors

Readers

  • Combustion science or combustion engineering.
  • Electrochemical Engineering/ Fuel Cell Technologies