Process Engineering Design for Manufacture of Guanidine Nitrate. Volume II

Abstract

The report completes the technical, operating and economic studies for a 3-year pilot plant demonstration of the urea/ammonium nitrate (U/AN) route to guanidine nitrate (GN) as an intermediate for manufacture of nitroguanidine (NQ). It summarizes the 1973 effort, including plant modifications, production of 10 tons of specification GN, economic comparison of the U/AN and British Aqueous Fusion (BAF) processes for GN, and layaway of the GN pilot plant. An economic catalyst (Houdry CP-532 silica bead) lifetime was shown in the reactors which are basically production prototypes in design and size. The concept of the U/AN process for manufacturing GN via a melt reactor plus a single aqueous crystallization step was demonstrated.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1973
Accession Number
AD0772074

Entities

People

  • J. A. Doyle
  • J. A. Gorton
  • M. G. Whippen
  • N. W. Steele

Tags

Communities of Interest

  • Biomedical
  • Ground and Sea Platforms
  • Human Systems

DTIC Thesaurus Topics

  • Chemical Analysis
  • Chemical Synthesis
  • Chemistry
  • Continuous Chemical Reactors
  • Control Systems
  • Dermatologic Agents
  • Economic Analysis
  • Engineering
  • Engineers
  • Industrial Plants
  • Management Personnel
  • Manufacturing
  • Material Degradation Processes
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Pilot Plants

Readers

  • Agricultural Chemistry/Soil Science
  • Industrial Economics
  • Rocket Propulsion.