Basic Research to Develop Selective Nuclear Magnetic Resonance Shift Reagents.
Abstract
The use of iron phthalocyanine, PcFe, as a shift reagent for unhindered amines was further explored. In addition work with the shift reagents PcFe(NH2C4H9)2 and PcFe(ND2C4D9)2 was carried out. These reagents were found to be effective and easy-to-use reagents for unhindered amines. Also done was work with the shift reagents PcFe(NH2C6H5)6 and PcFe(ND2C6D5)6. Of the reagents examined the latter appeared to be the best. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Apr 12, 1974
- Accession Number
- AD0783294
Entities
People
- Malcolm E. Kenney
Organizations
- Case Western Reserve University