STUDIES OF THE BREAKDOWN MECHANISM OF POLYMERS. 3. THE THERMAL DECOMPOSITION OF AROMATIC POLYAMIDES AND POLYIMIDES

Abstract

The breakdown mechanism of an aromatic polyamide and four polyimides has been studied. The decomposition of the polyamide in the temperature range below 375deg, C yield predominantly carbon dioxide, while between 375 and 450 deg C abo ut equal amounts of carbon dioxide and carbon monoxide formed. Hydrogen is the major product between 450 and 550 deg C, along with hydrogen cyanide, methane, and carbon monoxide. The major reaction at the lower temperatures seems to be the cleavage of the linkage between the carbonyl group and the ring, with subsequent formation of a carbodiimide linkage via isocyanate intermediates. At higher temperatures, cleavage between the carbonyl and the - NH- group takes place.

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1968
Accession Number
AD0833785

Entities

People

  • Gerhard F. L. Ehlers
  • Kurt R. Fisch
  • Wilbert R. Powell

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Air Force
  • Air Force Facilities
  • Carbon Dioxide
  • Carbon Monoxide
  • Chemistry
  • Composite Materials
  • Decomposition
  • Dielectric Gases
  • Films
  • Governments
  • Hydrogen Cyanide
  • Infrared Spectroscopy
  • Mass Spectroscopy
  • Materials
  • Materials Laboratories
  • Spectra
  • Spectroscopy

Readers

  • Organic Chemistry
  • Surface Coatings Technology.