DEVELOPMENT OF A SUBSCALE MANUFACTURING PROCESS FOR THE FABRICATION OF HYPEREUTECTIC TRANSITION-METAL CARBIDE COMPOSITES.

Abstract

Consumable-electrode arc melting and nonconsumable-electrode skull arc melting were investigated as possible manufacturing processes for the preparation of hypereutectic zirconium and hafnium carbide alloys. Variables in these processes were examined in detail. Forty-two experimental consumable-electrode runs resulting in castings up to 5 inches in diameter were performed. Techniques for preparing satisfactory castings up to 3-1/2 inches in diameter by this latter process were developed. The developed process consisted of two steps: prealloying and drop-casting. These steps are described. Over 1500 skull arc melting and casting runs were performed which yielded castings suitable for over 175 environment test specimens and 275 property test specimens. Thermal-conductivity, thermal-expansion, and heat-capacity measurements were made on specimens of ZrC+C alloys (19.7 to 24.4 wt % carbon) over the temperature range 70 to 4500 F and of HfC+C alloys (13.5 to 15.8 wt % carbon) over the temperature range 70 to 5000 F. Tensile tests, compression tests and dynamic-modulus measurements were also performed on these alloys at 70, 3500, and 4500 or 5000 F. Data obtained in these measurements are presented. (Author)

Document Details

Document Type
Technical Report
Publication Date
Sep 01, 1968
Accession Number
AD0841550

Entities

People

  • D. P. Moak
  • E. L. Foster Jr.
  • S. G. Nelson

Organizations

  • Battelle Memorial Institute

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Arc Melting
  • Casting (Fabrication)
  • Castings
  • Conductivity
  • Diameters
  • Drop Casting
  • Electrodes
  • Fabrication
  • Heat Capacity
  • Heat Energy
  • Manufacturing
  • Material Forming Processes
  • Measurement
  • Melting
  • Thermal Conductivity
  • Thermal Expansion
  • Transition Metals

Fields of Study

  • Materials science

Readers

  • Metallurgy
  • Surface Engineering/Surface Coating Technology.
  • Thermal Physics or Thermal Science.