Kinetics and Mechanisms of the Slow Decomposition of Some Model Explosive Compounds.

Abstract

Three model solid explosives of the N-aryl-N'-tosyloxydi-imide N-oxide system were thermally decomposed in the beam of an infrared spectrophotometer. Quantitative data from the infrared spectrograms were used to construct decomposition versus time curves. Rate constants were found from the curves, and these were used in turn to determine Arrhenius activation energies and frequency factors. A simple kinetic model was formulated so the Arrhenius values could be associated with plausible physical and chemical processes. Mathematical and experimental techniques were developed for studying continuous reactions in the solid state by infrared spectroscopy. (Author)

Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1969
Accession Number
AD0856714

Entities

People

  • Clelland R. Downs

Organizations

  • Air Force Institute of Technology

Tags

Communities of Interest

  • Counter IED
  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Analyzers
  • Chemical Reaction Properties
  • Chemical Reactions
  • Decomposition
  • Energy
  • Explosives
  • Frequency
  • Heat Of Activation
  • Infrared Spectrophotometers
  • Infrared Spectroscopy
  • Instrumentation
  • Kinetics
  • Measuring Instruments
  • Optical Equipment
  • Optical Instruments
  • Spectrophotometers
  • Spectroscopy

Readers

  • Computational Modeling and Simulation
  • Electrochemical Engineering/ Fuel Cell Technologies
  • Spectroscopy.