Perfluoroalkylene Oxide Polymers as High-Temperature Sealants

Abstract

Photolysis of perfluoroether diacid fluorides and chain-extension of fluorocarbonether-bridged chlorosilanes have been investigated as routes to a high-temperature integral fuel tank sealant polymer. Six different fluorocarbon ether-bridged chlorosilanes have been prepared and their polymerization to silanol-ended fluorccarbon ether-bridged siloxanes investigayed. Sealant compounds prepared from the siloxane polymers have long term stability in air up to 400 F. Substitution of trifluoropropyl groups on silicon is necessary to achieve the desired jet fuel resistance. Aging of two sealant compounds containing trifluoropropyl groups on silicon indicate that they will be useful for certain periods of time up to 500 F in a jet fuel environment. However, more research is necessary to firmly determine the upper temperature limit.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1970
Accession Number
AD0875022

Entities

People

  • James H. Jansen
  • James R. Throckmorton
  • Merritt L. Stigen
  • Paul H. Ogden

Organizations

  • 3M

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Chemical Products
  • Chemical Reactants
  • Chemical Reaction Properties
  • Composite Materials
  • Decomposition
  • Fuel Tanks
  • Fuels
  • High Temperature
  • Jet Engine Fuels
  • Material Degradation Processes
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Molecular Weight
  • Polymers
  • Silicon Compounds
  • Sodium Compounds

Fields of Study

  • Chemistry

Readers

  • Polymer Science and Engineering.