Chemistry of Catenated Nitrogen Compounds.
Abstract
Studies were conducted on the preparation and characterization of triazanium salts. A method was devised for synthesis of 2,2-dimethyltriazanium sulfate. The sulfate was converted to its perchlorate and nitrate by metathetical reactions. The isomer 1,1-dimethyltriazanium bisulfate was also prepared, but its conversion to the perchlorate was not successful. Triazanium bisulfate and methylsulfonate were prepared and characterized by ir spectroscopy. A hydrated triazanium perchlorate was apparently prepared, but attempts to obtain the anhydrous salt gave only decomposition products. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Apr 01, 1972
- Accession Number
- AD0893148
Entities
People
- Louis R. Grant