Thermochemistry and Reactivity of Metals Engaged in Chemiionization

Abstract

The exothermicity of the chemi-ionization reaction Sm + O -> SmO+ + e has been re evaluated. Guided ion beam tandem mass spectrometry (GIBMS) has been used to determine a value for the bond dissociation energy of SmO+ of 5.73 +/- 0.07 eV, as determined by the observed reactivity of Sm+ and SmO+ with several species. Combined with the established Sm ionization energy, this value indicates an exothermicity of the chemi-ionization reaction of 0.08 +/- 0.07 eV, ~0.2 eV smaller than previous literature determinations. This value agrees well with 0.14 +/- 0.17eV, independently determined from a new measurement of the ionization energy of SmO using resonantly enhanced two-photon ionization (REMPI) and pulsed-field ionization zero kinetic energy (PFI-ZEKE) photoelectron spectroscopy, 5.7427 +/- 0.0006 eV, combined with literature bond energies of SmO. The evaluated thermochemistry also suggests that D0(SmO) = 5.83 +/- 0.07 eV, consistent with but more precise than literature values. Implications of these results for interpretation of chemical release experiments in the thermosphere were evaluated.

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Document Details

Document Type
Technical Report
Publication Date
Dec 03, 2015
Accession Number
AD1000769

Entities

People

  • Peter B. Armentrout

Organizations

  • University of Utah

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemistry
  • Dissociation
  • Electrons
  • Electrospray Ionization
  • Energy
  • Energy Transfer
  • Ion Beams
  • Ionization
  • Kinetic Energy
  • Mass Spectrometry
  • Measurement
  • Oxidation
  • Spectrometry
  • Spin-Orbit Interaction
  • Thermodynamics

Fields of Study

  • Chemistry

Readers

  • Geochemistry
  • Molecular Photonics/Laser Physics

Technology Areas

  • Microelectronics