ARO Research Instrumentation Program - IR Spectrometer Procurement

Abstract

This report details the procurement and integration of an infrared (IR) spectrometer (Thermo Scientific - Nicolet iS50R Spectrometer) intoour electrochemistry program. The instrument is being utilized to characterize ionic liquid-based (IL-based) electrolyte systems viasimultaneous electrochemical and spectroscopic studies. These studies are enabling us to understanding the microscopic (molecular andionic) dynamics at electrolyte/electrode interfaces. This information is important for the development of enhanced energy conversionprocesses and devices (e.g., supercapacitors). The Nicolet iS50R spectrometer has been synchronized with a potentiostat to perform surfaceenhanced infrared absorption (SEIRA) spectroscopy during electrochemical (voltammetric) perturbation. The spectrometer has also beenutilized to help us characterize biomaterials before and after processing in a separate project that aims to create robust, functionalbiocomposites. In particular, we are interested to develop tough bio-based composites for energy storage and water remediationapplications. Sample data from these ongoing efforts are demonstrated in this report.

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Document Details

Document Type
Technical Report
Publication Date
Nov 01, 2015
Accession Number
AD1008598

Entities

People

  • Luke M. Haverhals

Organizations

  • Bradley University

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Synthesis
  • Chemistry
  • Department Of Defense
  • Electrodes
  • Electrolytes
  • Electron Microscopy
  • Energy Storage
  • Engineering
  • Films
  • Geometry
  • Ionic Liquids
  • Materials
  • Materials Science
  • Metal Films
  • Students
  • Surface Plasmon Resonance
  • Surface Plasmons

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Image Processing and Computer Vision.
  • Nanocomposite Materials Science