Improving Ion Mobility Spectrometry Detection Methods for Trace Forensics and Military Field Applications

Abstract

Ion mobility spectrometry (IMS) is a proven technology for field portable detection of vapor phase explosive compounds due to its high sensitivity and rapid analysis. However, IMS technology is limited in identifying complex samples in the field due to poor resolution and limited dynamic range. Combining gas chromatography (GC) to IMS can overcome some of the limitations by separating the components in a mixture before detection; however, the addition of GC increases system complexity and lengthens analysis times. The performance characteristics of the IMS and GC/IMS operational modes of the GC-IONSCAN were evaluated to determine if GC/IMS is more reliable than IMS in the detection of explosive compounds amidst interferents. Five explosive compounds (HMTD, PETN, RDX, TATP, and TNT) and four were used.

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Document Details

Document Type
Technical Report
Publication Date
Oct 11, 2016
Accession Number
AD1014216

Entities

People

  • Greg W. Cook

Organizations

  • Uniformed Services University of the Health Sciences

Tags

Communities of Interest

  • Biomedical
  • Counter IED
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemical Analysis
  • Chemical Compounds
  • Chemical Synthesis
  • Chemical Warfare Agents
  • Chemistry
  • Commercial Aviation
  • Explosions
  • Explosive Devices
  • Explosives
  • Explosives Detection
  • Health Services
  • Liquid Chromatography
  • Mass Spectrometry
  • Materials Laboratories
  • Materials Science
  • Materials Testing
  • Organic Chemistry

Readers

  • Agricultural Chemistry/Soil Science
  • Sensor Fusion and Tracking Systems.
  • Systems Analysis and Design