HAPSITE (registered trademark) Gas Chromatograph/Mass Spectrometer (GC/MS) Variability Assessment

Abstract

The need for rapid response chemical detection instruments has received a great deal of attention in the post-September 11 world [Belke, 2004]. It is critical that first-response personnel be able to characterize the chemical hazards associated with a response. A military response, accident or act of terror is already a stressful situation but the situation becomes much more challenging in an uncharacterized chemical environment that involves chemical warfare agents (CWA) or toxic industrial chemicals (TIC). Gas Chromatography/Mass Spectrometry (GC-MS) technology can provide the ability to characterize and identify unknown chemicals during an emergency situation. Identifying unknown chemicals enables authorities to take more precise steps necessary to protect the population and incident responders for the specific hazard. GC-MS provides the ability to quantify the concentration of the chemicals present and thus the specific health risk posed by the chemicals [Nation Institute of Justice, 2000]. In the past, GC-MS systems were operated only in a controlled laboratory setting where wet chemistry procedures could be performed and bulky supplies such as compressed gas cylinders were readily available. The traditional sampling and analysis methods, using lab based GC-MS, function well for, non-emergency situations but are too time consuming when information is needed quickly. With the traditional method, extensive time is required to collect the unknown air sample onto a sorbent media (typically a tube filled with activated charcoal), package and ship the sample to a lab for analysis. There is a need to take the GCMS technology into the field for rapid chemical identification at a response scene.

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Document Details

Document Type
Technical Report
Publication Date
Jun 09, 2004
Accession Number
AD1014554

Entities

People

  • Michael A. Skinner

Organizations

  • Uniformed Services University of the Health Sciences

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Air Force
  • Alkenes
  • Chemical Compounds
  • Chemical Synthesis
  • Chemical Warfare
  • Chemical Warfare Agents
  • Chemistry
  • Gas Chromatography
  • Mass Spectrometers
  • Mass Spectrometry
  • Measurement
  • Organic Chemistry
  • Organic Compounds
  • Spectrometers
  • Spectrometry
  • Test Methods
  • Volatile Organic Compounds

Readers

  • Analytical Chemistry
  • Emergency Management and Homeland Security.
  • Environmental Engineering.