Development of Advanced Li Rich xLi2MO3 (1-x)LiMO2 Composite Cathode for High Capacity Li Ion Batteries

Abstract

Recently, lithium-rich layered oxides have become attractive cathode materials for high torage energy applications. Lithium rich layered oxides materials, represented by the general formula xLi2MnO3(1 - x)LiMO2 in which M is MnNi and Co are of interest for both high-power and high capacity lithium ion cells. In this study, a series of cathode materials with chemical formula of xLi2MnO3(1-x)LiNi1/3Mn1/3Co1/3O2 (x = 0, 0.3, 0.5, 0.7and 1.0) were synthesized by solgel method and investigated for their structure and electrochemical properties. The crystal structure of the sample was examined by X-ray diffraction. It is found that xLi2MnO3(1-x)LiNi1/3Mn1/3Co1/3O2 possessed the composite characteristic of two relatively similar layered structures. Its electrochemical performance is examined with galvanostatic charge/discharge. Increasing Li2MnO3 content tends to stabilize Li rich structure to increase capacity. On the other hand, Li2MnO3 shows an irreversible reaction with a reduced capacity. Accordingly, an optimized result was obtained from 0.5Li2MnO30.5LiNi1/3Mn1/3Co1/3O2 cathode which shows highest electrochemical performance with discharge capacity of 250 mAh/g. However, the capacity fading from these materials was also observed. To understand the behavior of capacity fading for Li-rich cathode materials, Li[Li0.2Mn0.54Ni0.13Co0.13]O2 as a cathode material for Li-ion battery has been carefully investigated. The result shows high initial charge capacity of 327 mAh/g and discharge capacity of 276 mAh/g at 0.05C rate (15mA/g) respectively. After 30 cycles, the discharge capacity decayed to 169 mAh/g. Transmission electron microscopy (TEM) images

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Document Details

Document Type
Technical Report
Publication Date
Dec 22, 2016
Accession Number
AD1027334

Entities

People

  • Chia-chin Chang
  • Kuan-zong Fung
  • Ying S. Meng

Organizations

  • National Cheng Kung University

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Air Force Research Laboratories
  • Chemistry
  • Composite Materials
  • Diffraction
  • Electrodes
  • Electron Microscopes
  • Electron Microscopy
  • Energy
  • Energy Storage
  • Materials
  • Materials Science
  • Microscopy
  • Particle Size
  • Phase Transformations
  • Photoelectrochemical Cells
  • Transition Metals
  • Transmission Electron Microscopy

Fields of Study

  • Materials science

Readers

  • Battery Technology and Engineering
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics