Tunable Artificial Receptor as a Chemical Sensor for V- and G-agents

Abstract

Battelle investigated the development of a tunable artificial receptor designed with a sliding ring ( e.g., Host-[2]rotaxane) that detects the presence of V- and G- nerve agents. The ultimate purpose for this work is to develop a tunable hazard mitigation system capable of capturing, detecting, and destroying chemical agents. Agent capture occurs by the receptor's use of two cooperative non-covalent interactions: hydrophobic binding and salt-bridging. Agent capture efficiency was evaluated using Soman (GD). GD was effectively bound in water at I 0-5 M demonstrating the potential ability to sequester GD for subsequent decontamination. Computational studies were performed by modeling docking interactions using EPP, GA, and GD to understand the nature of the binding motifs. Two binding motifs are suggested for the EPP complex, a "phenyl-in" and an "ethyl-in" mode. The phenyl group inside the cyclophane is significantly more strongly bound than the EPP complex with the ethyl group inside the cyclophane. Both binding motifs show stable binding energies ranging from O - 5 kcal/mol which is expected for hydrophobic interactions. This finding supports the cross-over use of cyclophanes as design elements for capturing chemical agents in artificial receptor systems.

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 2012
Accession Number
AD1043036

Entities

People

  • Donald Ii W Zehnder
  • John R Shaw

Organizations

  • Battelle Memorial Institute

Tags

Communities of Interest

  • Energy and Power Technologies
  • Sensors

DTIC Thesaurus Topics

  • Chemical Synthesis
  • Chemical Warfare
  • Chemical Warfare Agents
  • Chemistry
  • Computational Science
  • Dermatologic Agents
  • G Agents
  • Liquid Chromatography
  • Mass Spectrometry
  • Nerve Agents
  • Organic Chemistry
  • Sodium Compounds
  • Spectra

Readers

  • Computational Fluid Dynamics (CFD)
  • Nanocomposite Materials Science
  • Neurotoxicology