Removal of Perfluorinated Compounds from Post-Emergency Wastewater by Advanced Oxidation Process and Granular Activated Carbon Adsorption

Abstract

This research presents a novel approach to remove per- and polyfluoroalkyl substances (PFAS) from aqueous film-forming foam (AFFF) impacted wastewater with high (~100 mg/L) total organic carbon (TOC) concentrations. A treatment-train process was investigated involving an ultraviolet (UV)/hydrogen peroxide (H2O2) advanced oxidation process (AOP) followed by filtration using Calgon Filtrasorb 600 (F600) granular activated carbon (GAC). UV/H2O2 AOP experiments were conducted to determine whether TOC concentrations could be reduced as a pre-treatment step before filtering the water with F600-GAC. Results showed using UV/H2O2 AOP reduced TOC in solution by > 98%. Reducing TOC concentrations was achieved by using a 250 mg/L H2O2 concentration and operating the UV/H2O2 AOP system for 8-hours. Rapid small-scale column tests (RSSCT) were used to determine whether pre-treatment with AOP affects GAC adsorption capacity for PFAS, specifically perfluorooctane sulfonic acid (PFOS) and perfluorooctanoic acid (PFOA). The UV/H2O2 AOP pre-treatment process increased GAC capacity through 10% breakthrough (BV10) for PFOS by 1800% (increasing the adsorbents solid phase concentration from 3 mg-PFOS/g-GAC without pre-treatment up to > 52 mg-PFOS/g-GAC with pre-treatment). The pre-treatment process also improved BV10 GAC capacity for PFOA by 1100% (1.1 mg-PFOA/g-GAC up from 0.1 mg-PFOA/g-GAC) when operating the UV/H2O2 AOP for 8-hours versus two-hours.

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Document Details

Document Type
Technical Report
Publication Date
Mar 22, 2018
Accession Number
AD1056482

Entities

People

  • Sean M Dyson

Organizations

  • Air Force Institute of Technology

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Advanced Oxidation Processes
  • Air Force
  • Chemical Synthesis
  • Chemistry
  • Ecology
  • Environment
  • Environmental Exposure
  • Environmental Health
  • Environmental Monitoring
  • Environmental Pollutants
  • Environmental Protection
  • Groundwater
  • Hydrogen
  • Liquid Chromatography
  • Materials
  • Measurement
  • Water Purification

Fields of Study

  • Environmental science

Readers

  • Agricultural Chemistry/Soil Science
  • Internal Combustion Engine (ICE) Technology.