New Polymeric Materials Incorporating Heteromatic Phosphabenzene Units

Abstract

The proposed project described the incorporation of aromatic phosphorus heterocycles into polymer main chains and side chains. While pyridine and thiazole have been explored extensively in polymer chemistry, the phosphorus analogs (phosphinine and thiaphosphole) have yet to be incorporated into macromolecular structures. Monomer syntheses were explored for both ring systems and polymerization efforts resulted in some success for phosphinine-containing oligomers. Synthetic method development for both phosphinine and thiaphosphole proved challenging, and a successful efficient route to polymerizable monomers has not yet been established. Further efforts have looked at other phosphorus containing monomers in conjugated structures. This project has also been expanded to controlled polycondensation for semiconducting polymers. Furan, which is a bio renewable monomer, has been explored in controlled polycondensation. High molecular weights could not be achieved due to aggregation but the furan was incorporated into an alternating polymer with thiophene to obtain solution-processable materials.

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Document Details

Document Type
Technical Report
Publication Date
Sep 29, 2016
Accession Number
AD1063267

Entities

People

  • Kevin J T Noonan

Organizations

  • Carnegie Mellon University

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Abstracts
  • Agreements
  • Catalysts
  • Chemical Synthesis
  • Chemistry
  • Conjugated Polymers
  • Copolymers
  • Department Of Defense
  • Engineering
  • Macromolecules
  • Mass Spectrometry
  • Materials
  • Molecular Weight
  • Molecules
  • Oligomers
  • Organic Chemistry
  • Polymer Chemistry
  • Polymers
  • Spectra
  • Spectroscopy

Fields of Study

  • Chemistry

Readers

  • Polymer Science and Technology
  • Research Science/Academic Research