Development of a Multi-Frame Detection System to Obtain Real-Time X-Ray Measurements in Shocked Energetic Materials

Abstract

This DURIP award was used to acquire/assemble a Multi-frame Detection System to obtain real-time x-ray diffraction and phase contrast imaging measurements (micrometer resolution) in energetic materials (EMs) subjected to well-characterized shock wave loading. Such measurements will permit for the first time the ability to routinely examine changes in crystal structure (phase transformations), microstructure, and crystal-binder interfaces in real-time (while they are happening in nanoseconds to microseconds) in dynamically compressed EMs. The importance/relevance of such measurements for fundamental research, and for the safe and optimal use of EMs, cannot be emphasized enough. X-ray diffraction and phase contrast imaging measurements will not only provide new mechanistic insights into EM response, but will also serve to evaluate multiscale modeling results. The multi-frame detection system is deployed at the Dynamic Compression Sector (DCS) located at the Advanced Photon Source (Argonne), a first-of-its-kind user facility dedicated to dynamic compression science. Having this multi-frame detector capability (for x-ray diffraction and imaging) available for dynamic experiments on EMs provides a novel and unique experimental capability for the Office of Naval Research and other Department of Defense research related to EMs. X-ray diffraction and imaging measurements on dynamically compressed EMs have not been possible before. In addition, a new generation of research scientists will be educated on using such facilities for EM related research.

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Document Details

Document Type
Technical Report
Publication Date
Nov 27, 2018
Accession Number
AD1063896

Entities

People

  • Yogendra Gupta

Organizations

  • Washington State University

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Reactions
  • Crystal Structure
  • Crystals
  • Department Of Defense
  • Detection
  • Diffraction
  • Energetic Materials
  • Explosives
  • High Explosives
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Measurement
  • Plastic Bonded Explosives
  • Subatomic Particles
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Physics

Readers

  • Electromagnetic Wave Scattering and Antenna Radiation Engineering
  • Image Processing and Computer Vision.
  • Research Science/Academic Research