Final Report: Insights in catalytic transformations at the solid-liquid interface using MES-ATR-IR Spectroscopy

Abstract

Getting molecular-level insights into processes at solid interfaces is a highly challenging task. In this work, we use Modulation Excitation Spectroscopy in combination with Infrared Spectroscopy to gain such insights on solid-liquid and solid-gas interfaces. We studied the cyclization of citronellal and the coupling of ethanol forming butadiene as case studies of reactions of contemporary interest to further develop the technique, the setups and test its applicability. We obtained intriguing results that helped us propose molecular-level reaction mechanisms that rationalize literature data. This work has lead to two publications in peer-reviewed journals and allowed us to further advance the technique.

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Document Details

Document Type
Technical Report
Publication Date
Aug 12, 2016
Accession Number
AD1064213

Entities

People

  • Ive Hermans
  • Philipp Mueller

Organizations

  • University of Wisconsin–Madison

Tags

Communities of Interest

  • Human Systems

DTIC Thesaurus Topics

  • Alcohols
  • Alkenes
  • Butadienes
  • Catalysis
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Engineering
  • Infrared Spectroscopy
  • Liquid Phases
  • Mass Spectrometers
  • Mass Spectrometry
  • Phase Studies
  • Spectra
  • Spectroscopy
  • Students
  • Temperature Gradients

Readers

  • Nanoscale Plasmonic Nanotechnology
  • Quantum Chemistry
  • Technical Research and Report Writing.