A Mechanochemistry-Based Technique For Early Material Damage Detection In High Strain Rate Processes

Abstract

It is often desired to detect damage at the sub-continuum level before continuum-level damage is observed. The burgeoning field of polymer mechanochemistry promises development of novel materials that would report sub-continuum-level damage if a critical stress or strain level is exceeded. In addition, a long-standing challenge for multi-scale modeling validation has been the generation of experimental data to link molecular-level damage to macroscopic material behavior at high rate. Using mechanophore-embedded silicone elastomer samples, for the first time ever, molecular-level bond breakage is captured visually during standard high-rate material characterization experiments, prior to the onset of macroscopic damage. A brief description of synthesized mechanophores, methods of embedding into the silicone elastomer, and the method to determine the critical strain of mechanophore activation (molecular-level bond breakage) is included. The critical strain and critical stress values are determined for the onset of molecular-level bond breakage. Constitutive models enhanced with the method presented in this report can potentially be used for validation of multi-scale material failure computational model development efforts to simulate ballistic impact events. The results reported herein contribute to the investigations of mechanophore-embedded materials for enhanced stress assessment and for the development of mechanophore-based adaptive/multifunctional protection materials.

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Document Details

Document Type
Technical Report
Publication Date
Jan 30, 2019
Accession Number
AD1067076

Entities

People

  • Daniel Casem
  • James Berry
  • Logan Shannahan
  • Meredith H Barbee
  • Müge Fermen-coker
  • Stephen L Craig
  • Yangju Lin

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Biomedical
  • Human Systems
  • Weapons Technologies

DTIC Thesaurus Topics

  • Alkanes
  • Alkenes
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Damage Detection
  • Detection
  • Elastomers
  • Fungi
  • Materials
  • Materials Science
  • Mechanical Properties
  • Molecules
  • Organic Chemistry
  • Polymers
  • Strain Rate
  • Three Dimensional

Readers

  • Polymer Science and Engineering.
  • Quantum Chemistry
  • Systems Analysis and Design