Characterization of Solid Reaction Products from the Reaction of VX with Li3N+H2O for the Tactical Disablement Project

Abstract

As part of the Tactical Disablement Project, 100 mL of neat weapons-grade omicron-ethyl-S-(2-diisopropylaminoethyl) methyl phosphonothiolate (VX) was reacted with 8 g of lithium nitride (Li3N) and 10 g of water in a glass reaction vessel. The addition of the water and Li3N resulted in an approximately 16 increase in the volume of the reaction. Products were analyzed, and reaction schemes are provided to explain the products. The observed products are consistent with previous studies of VX reactions in caustic decontamination solution, forming primarily VX acid (ethyl methylphosphonic acid) and VX disulfide [bis(2-diisopropylaminoethyl) disulfide].

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Document Details

Document Type
Technical Report
Publication Date
Feb 24, 2020
Accession Number
AD1091850

Entities

People

  • David J. Mcgarvey
  • Mark K. Kinnan
  • William R. Creasy

Organizations

  • United States Army Soldier Systems Center

Tags

Communities of Interest

  • Counter WMD
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Analytical Chemistry
  • Analytical Chemistry Techniques
  • Batch Reactors
  • Chemical Shifts
  • Chemical Synthesis
  • Chemical Warfare
  • Chemical Warfare Agents
  • Chemistry
  • Decontamination
  • Liquid Chromatography
  • Magnetic Resonance
  • Mass Spectra
  • Mass Spectrometry
  • Nuclear Magnetic Resonance
  • Raman Spectra
  • Raman Spectroscopy
  • Reaction Time
  • Spectra
  • Spectrometry
  • Spectroscopy
  • Standards

Readers

  • Analytical Chemistry
  • Chemistry (specifically Chemical Fluorescence)