Electrospun Composite Membranes for Alkaline Fuel Cells

Abstract

Electrospun fiber composite anion exchange membranes were created by electrospinning two polymers: a chloromethylated polysulfone that would ultimately serve as the hydroxide ion conductor, and an uncharged polyphenylsulfone to limit water swelling and provide mechanical strength to the final membrane. After electrospinning, the chloromethyl groups were converted into quaternary ammonium moieties for hydroxide ion conduction. The polyphenylsulfone fibers were then selectively made to flow and fill the void space in the dual fiber mat, thus forming a dense, defect free membrane. The final membrane morphology was a quaternized polysulfone interconnecting fiber network embedded in a polyphenylsulfone matrix. For a membrane containing 63 vol percent anion-exchange polymer fibers (with a fiber IEC of 2.5 mmol g-1), the OH- ion conductivity was high (40 mS cm-1 in 23 deg C water) and the equilibrium water swelling at room temperature was low (70 vol percent).

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Document Details

Document Type
Technical Report
Publication Date
Dec 09, 2015
Accession Number
AD1092150

Entities

People

  • A. M. Park
  • P. N. Pintauro

Organizations

  • Vanderbilt University

Tags

Communities of Interest

  • Advanced Electronics
  • Air Platforms

DTIC Thesaurus Topics

  • Abstracts
  • Alkaline Fuel Cells
  • Cells
  • Chemistry
  • Composite Materials
  • Fibers
  • Films
  • Fuel Cells
  • Hydrogen
  • Hydroxides
  • Ion Exchange
  • Liquids
  • Materials
  • Mechanical Properties
  • Polymers
  • Spectra
  • Water

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Reinforced Composite Materials
  • Underwater engineering and Marine Technology.

Technology Areas

  • Biotechnology
  • Space
  • Space - Hall-Effect Thruster