Study of Advanced Thermal Barrier Coatings and Calcia-Magnesia-Alumino-Silicate (CMAS) Interactions

Abstract

The infiltration and adhesion of molten particulates is a significant problem for gas-turbine engines (GTEs) operating in particle-laden environments. The resultant glassy calcia-magnesia-alumino-silicate coating on hot-section components can lead to early GTE failure and decreased rotorcraft flight time. Between 2000 and 2013, the US military lost 26 rotorcraft, costing $533 million, due to operating in brownout conditions. A quantitative understanding of the chemical reaction kinetics between ingested particulates and thermal barrier coatings (TBCs) is key to developing effective mitigation strategies that limit Army exposure to this environmental risk. To this end, we have mixed TBC powders with a synthetic sand, AFRL-02, to study the reaction kinetics. After analysis with a scanning electron microscope (SEM), equipped with an energy-dispersive X-ray spectrometer (EDS) for elemental analysis, the powders were melted at 1,300 C for 4 h. The resultant glass was subsequently imaged/analyzed with SEM-EDS. In addition, X-ray diffraction and differential scanning calorimetry (up to 1,400 C) data are also being collected on the powder mixtures to aid in identifying new phases and reactive species being formed. The information will be used to develop new TBCs with sandphobic qualities for increased reliability/durability of Army vertical-takeoff-and-landing engines.

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 2020
Accession Number
AD1109556

Entities

People

  • Alex Berendt
  • Anindya Ghoshal
  • Michael Walock
  • Muthuvel Murugan
  • Rick Reidy

Organizations

  • United States Army Combat Capabilities Development Command

Tags

DTIC Thesaurus Topics

  • Abstracts
  • Adhesion
  • Barrier Coatings
  • Ceramic Matrix Composites
  • Chemical Kinetics
  • Chemical Reactions
  • Chemistry
  • Coatings
  • Composite Materials
  • Department Of Defense
  • Electron Microscopes
  • Engines
  • Gas Turbines
  • Information Operations
  • Instructions
  • Kinetics
  • Military Research
  • Particle Size
  • Particles
  • Rotary Wing Aircraft
  • Scanning Electron Microscopes
  • Silicon Carbide
  • Standards
  • Turbine Components
  • Turbines
  • Vertical Takeoff Aircraft
  • X Rays
  • X-Ray Diffraction

Readers

  • Powder metallurgy of Titanium alloys.
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Microelectronics