Zirconium Hydroxide Nanoparticles for Toxic Chemical Sequestration: Environmental Implications on Surface Reactivity, Capacity, and CWA Decomposition

Abstract

The objective of this project was to understand how operando conditions, such as common atmospheric contaminants and environmentalconditions like light and temperature, affect the adsorption and decomposition mechanisms of CWAs and CWA simulants on zirconium hydroxide, a promising sorbent and decomposition material. Decomposition of simulants and CWAs were studied primarily using ambient-compatible and soft characterization methods such as ATR-IR, DRIFTS, microbreakthrough, and XPS. Theoretical calculations provide experimental support and insight into most likely decomposition pathways, adsorbate stability, and potential surface poisoning resulting from decomposition products.

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Document Details

Document Type
Technical Report
Publication Date
Dec 03, 2020
Accession Number
AD1116840

Entities

People

  • Christopher J. Karwacki
  • Craig K. Knox
  • Daniel E Barlow
  • Grant C. Daniels
  • Gregory W. Peterson
  • Igor V Schweigert
  • Ivan Iordanov
  • James H Wynne
  • Jeffrey G Lundin
  • Lennart D Gunlycke
  • Monica L McEntee
  • Pehr E. Pehrsson
  • Robert B Ballow
  • Seokmin Jeon
  • Spencer L. Giles
  • Victor Bermudez
  • Wesley O Gordon

Organizations

  • United States Naval Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies
  • Engineered Resilient Systems

DTIC Thesaurus Topics

  • Chemical Analysis
  • Chemical Engineering
  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemical Synthesis
  • Chemical Warfare
  • Chemical Warfare Agents
  • Chemistry
  • Computational Chemistry Methods
  • Dielectric Gases
  • Electrodeposition
  • Linear Accelerators
  • Mass Spectrometry
  • Materials
  • Materials Science
  • Organic Chemistry
  • Spectra
  • Spectrometry
  • Spectroscopy
  • Surface Chemistry
  • Surface Properties

Fields of Study

  • Environmental science

Readers

  • Analytical Chemistry
  • Electrochemical Engineering/ Fuel Cell Technologies
  • Nanocomposite Materials Science

Technology Areas

  • Biotechnology