Evaluation of Indirect Thermal Desorption Coupled with Thermal Oxidation Technology to Treat Solid PFAS-Impacted Investigation-Derived Waste

Abstract

Previous studies have shown that thermal technology can reduce levels of per- and polyfluoroalkyl substances (PFAS) in soil, combust PFAS contained in commercial products, or mineralize PFAS-based industrial chemicals. However, uncertainties remain regarding ITD parameterization for application to treatment of specific PFAS-impacted waste as well as the destruction and removal efficiency (DRE) that can be achieved through off-gas treatment by thermal oxidation (TO). The overall objective of this study was to advance the current understanding of ITD/TOs effectiveness for the treatment of soil containing a typical suite of PFAS found in, but not limited to, aqueous film forming foam (AFFF) formulations manufactured and heavily utilized prior to 2002.A series of ten tests were conducted on sand spiked with PFAS at concentrations ranging from approximately 6,000 to 19,000 micrograms per kilogram (g/kg). Spiked feed soil samples and thermally treated soil samples were collected for each test run. Soil samples were collected in duplicate for each condition. Over 60 soil samples were collected. All soil samples were analyzed for PFAS using U.S. Environmental Protection Agency (EPA) Method 537 Liquid Chromatography/Tandem Mass Spectrometry. For the test runs spiked with AFFF, soil samples were also analyzed for Total Oxidizable Precursor Assay.

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Document Details

Document Type
Technical Report
Publication Date
Feb 01, 2020
Accession Number
AD1134384

Entities

People

  • Frank Barranco
  • George Hay
  • Paul Caprio

Tags

DTIC Thesaurus Topics

  • Air Force
  • Chemical Analysis
  • Chemical Synthesis
  • Chemistry
  • Combustion
  • Department Of Defense
  • Detection
  • Detectors
  • Ecology
  • Environmental Protection
  • Exhaust Gases
  • Flow Rate
  • Gas Flow
  • Gas Meters
  • Hydrogen
  • Hydroxides
  • Liquid Chromatography
  • Liquids
  • Materials Laboratories
  • Materials Testing
  • Measurement
  • Performance Tests
  • Pitot Tubes
  • Soil Tests
  • Test Methods
  • Water

Fields of Study

  • Environmental science

Readers

  • Agricultural Chemistry/Soil Science
  • Analytical Chemistry
  • Fire Suppression Systems Design.