Imidazolium Perchlorate: A Novel Energetic Molecular Ferroelectric

Abstract

We have investigated the changes in structure, composition, and microsecond-timescale energy release behavior for a molecular ferroelectric salt, imidazolium perchlorate (ImClO4), as a function of polarization. Low-temperature heating sufficient to depolarize the ImClO4 results in desorption of imidazole rings and significant morphological changes at the atomic scale but does not influence the microsecond-timescale energy release. Higher temperature pyrolysis at 350 degrees C produces a large exotherm and gas-combustion products such as H2O, CO/N2, and CO2. The estimated detonation velocity measured via the laser-induced air shock from energetic materials method was 7.2 km/s, which is comparable to the military explosive hexanitrostilbene. Despite its relatively unfavorable oxygen balance (43 percent), the ferroelectric properties of ImClO4 may make it suitable for specialized energetic applications.

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 2021
Accession Number
AD1147919

Entities

People

  • Chi-chin Wu
  • Jennifer L Gottfried
  • Rose A. Pesce-rodriguez
  • Scott D. Walck
  • Shenqiang Ren

Organizations

  • United States Army
  • University at Buffalo

Tags

Communities of Interest

  • Advanced Electronics
  • Counter IED
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Ammonium Perchlorate
  • Chemical Analysis
  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Combustion
  • Composite Materials
  • Curie Temperature
  • Dielectrics
  • Energetic Materials
  • Exothermic Reactions
  • Explosives
  • High Explosives
  • Mass Spectra
  • Materials
  • Materials Laboratories
  • Materials Science
  • Microelectromechanical Systems
  • Petn
  • Phase Transformations
  • Piezoelectric Crystals
  • Pyrolysis
  • Spectra
  • Spectroscopy

Readers

  • Materials Science and Engineering.
  • Molecular Photonics/Laser Physics
  • Rocket Propulsion.

Technology Areas

  • Directed Energy
  • Directed Energy - Lasers