A Spectroscopic Approach to Overcome the Barriers of Early Familial Hypercholesterolemia Diagnosis

Abstract

In diagnosing and treating familial hypercholesterolemia (FH) knowing both the good (HDL) and bad (LDL) cholesterol levels is extremely important as it allows a person to reduce the risk of heart disease and stroke. We propose to develop novel optical spectroscopy-based methods to cover the gap in FH diagnosis through use of surface-enhanced Raman spectroscopy (SERS). Our innovation is to use near infrared light (just outside the visible spectrum) and gold nanorods to measure LDL cholesterol more accurately and directly. We hypothesize that SERS spectra interpreted with quantum chemistry calculations and combined with the unique surface chemistry of gold nanorods will enable two critical advances in cholesterol detection for FH and other diseases. To test our hypothesis, we will 1) identify experimentally observable Raman vibrational modes for cholesterol detection and 2) test sensitivity of cholesterol detection in serum and in tissue. Major findings include that time dependent density-functional theory (TDDFT) calculations for the Raman vibrations of cholesterol show the presence of spectral bands of cholesterols tetracyclic rings which provide information on local chemical properties and experimentally, a SERS signal is detectable from surfactant coated nanorods when placed onto skin, which could enable new non-invasive tissue analysis methods for disease diagnosis.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 2023
Accession Number
AD1200772

Entities

People

  • Carly S Filgueira

Organizations

  • Houston Methodist Research Institute

Tags

DTIC Thesaurus Topics

  • Acquisition
  • Biomedical Research
  • Blood
  • Chemical Synthesis
  • Chemistry
  • Cholesterol
  • Density Functional Theory
  • Detection
  • Diseases
  • Health Services
  • Lipids
  • Medical Personnel
  • Membrane Lipids
  • Metallic Nanoparticles
  • Quantum Chemistry
  • Raman Scattering
  • Raman Spectra
  • Raman Spectroscopy
  • Scattering
  • Spectra
  • Spectroscopy

Readers

  • Electrochemical Surface Science
  • Prostate Cancer Biology.
  • Quantum Chemistry

Technology Areas

  • Quantum Computing