In-Situ Electron Microscopy of DNA-Guided Self Assembly and Reconfiguration of 3D Nanocrystal Superlattices

Abstract

Major Goals: Solution-phase self-assembly of nanoparticles into mesoscale structures via engineered nucleic acid linkers is a promising strategy for constructing functional materials and dynamically adaptive materials architectures from nanoscale components. Access to such systems is critical for realizing a wide range of defense-related capabilities including ultrasensitive surface-enhanced Raman scattering (SERS) detection of chemical or biological agents, manipulation of the electromagnetic spectrum and photonic cloaking, development of autonomous inorganic organisms, or novel approaches to quantum information processing. The microscopic processes governing DNA-mediated self-assembly and reconfiguration remain poorly understood. Conventional experimental approaches can assess only the final assembly outside the native solution environment or follow the degree of ordering but do not provide access to real-space pathways and dynamics in the native solution environment, especially at small scale. Nanometer-resolution imaging approaches have large potential to advance our understanding of DNA-guided nanoparticle assemblies, and can support the exploration and harnessing of their technological potential. Here we use real-time observations by in-situ liquid cell electron microscopy (LCEM) and complementary in-situ imaging approaches, coupled with numerical simulations in a research program aimed at establishing the fundamental mechanisms, pathways, and forces that govern DNA-guided nanoparticle self-assembly and dynamic reconfiguration in the native liquid environment.

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Document Details

Document Type
Technical Report
Publication Date
Jun 07, 2021
Accession Number
AD1202744

Entities

People

  • Eli Sutter
  • Peter Sutter

Organizations

  • University of Nebraska–Lincoln

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Aqueous Solutions
  • Aspect Ratio
  • Chemistry
  • Computer Simulations
  • Crystals
  • Electron Beams
  • Electron Microscopy
  • Materials
  • Materials Science
  • Microscopy
  • Nanotechnology
  • Particles
  • Radiation
  • Self Assembly
  • Spectroscopy
  • Surface Plasmon Resonance
  • Three Dimensional

Readers

  • Molecular Genetics
  • Nanoscale Plasmonic Nanotechnology

Technology Areas

  • Biotechnology
  • Microelectronics
  • Quantum Computing
  • Space
  • Space - Spacecraft Maneuvers