Evaluation of Novel Atypical Beta-Lactams Against Mycobacterial Ldt Enzymes Toward Combatting Antibiotic Resistance

Abstract

Antimicrobial resistance continues to grow as a global issue. This work aims to combat this concern by investigating L,D-transpeptidase (Ldt) enzymes as potential new drug targets using atypically modified Beta-lactam compounds. Ldts perform an essential function in formation of the peptidoglycan layer of mycobacterial cell walls. These unique Ldt enzymes provide an avenue of drug design by exploiting their essentiality in mycobacterial cell wall biosynthesis and nature specific to mycobacterial infections. There are six evolutionarily distinct classes of mycobacterial Ldts and different mycobacteria species may have all or varying numbers of Ldt classes present. Class 2 Ldts from various mycobacterial species - including that which causes tuberculosis - were the target in this study and were inactivated by both a commercial and synthetic carbapenem, imipenem and compound 10a respectively. Compound 10a is an atypically modified carbapenem, a subclass of beta-lactam, with demonstrated promise as a potential treatment. The two carbapenems of interest were evaluated based on their acylation kinetic profiles generated via stopped-flow tryptophan fluorescence and DynaFit non-linear regression software. Mass spectrometry data supported the nonlinear fits and rate constants produced by DynaFit software. Investigating the acylation kinetics of these compounds will further guide drug design studies toward identifying new Ldt inhibitors.

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Document Details

Document Type
Technical Report
Publication Date
May 16, 2023
Accession Number
AD1207067

Entities

People

  • Rachel E. Sanborn

Organizations

  • United States Naval Academy

Tags

DTIC Thesaurus Topics

  • Abstracts
  • Albumins
  • Amino Acids
  • Anti-Bacterial Agents
  • Anti-Infective Agents
  • Bacteria
  • Carrier Proteins
  • Cell Physiological Processes
  • Cells
  • Cellular Structures
  • Chemical Synthesis
  • Chemistry
  • Data Sets
  • Emission Spectra
  • Infection
  • Infectious Diseases
  • Mass Spectrometry
  • Microbiology
  • Monte Carlo Method
  • Mycobacterium Tuberculosis
  • Spectra
  • Spectrometry
  • United States
  • United States Naval Academy

Readers

  • Aquatic Ecology
  • Infectious Disease/Epidemiology
  • Microbial Pathology