Study of the Reaction of Cellulose Nitrate with Isocyanates

Abstract

Cellulose nitrate phenyl carbamate was synthesized and characterized. When studying the synthesis, it was discovered that it is not necessary to conduct this reaction under strictly anhydrous conditions. The reaction is aided by the excess of phenyl isocyanate, elevated temperatures, suitable solvents and a low degree of substitution of nitrocellulose. Denitration occurs as the reaction progresses; however, the formation of the carbamate substituent is not directly related to the loss of the nitrate groups.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 1975
Accession Number
ADA009506

Entities

People

  • Jack Bobinski

Organizations

  • Picatinny Arsenal

Tags

DTIC Thesaurus Topics

  • Absorption
  • Absorption Spectra
  • Acids
  • Alkanes
  • Boiling Point
  • Catalysts
  • Chemical Reaction Properties
  • Chemical Synthesis
  • Chemistry
  • Materials
  • Materials Science
  • Nitrocellulose
  • Polymerization
  • Propellant Grains
  • Propellants
  • Reaction Time
  • Solid Propellants

Fields of Study

  • Chemistry

Readers

  • Agricultural Chemistry/Soil Science
  • Organic Chemistry
  • Systems Analysis and Design