The Influence of Microstructure on Fracture of Ceramics

Abstract

A technique has been developed for the measurement of the viscosity of the amorphous phase in the grain boundaries of silicon nitride. The technique will serve as a useful tool in the development of these ceramics since a correlation can now be established between the viscosity of the grain-boundary phase and its chemistry. Some work has been completed on building models for intergranular fracture in these materials based upon the concept of fracture in a thin viscous adhesive layer sandwiched between two hard surfaces. A simple model which considers fracture by the growth of penny-shaped voids in the adhesive layer gives sensible agreement with actual fracture measurements in silicon-nitride at elevated temperatures. The relationship between yielding and fracture in semi-brittle ceramic crystals has also been investigated. Strengthening of I-VII compounds, e.g. KCl, NaCl, and LiF, by divalent impurity additions is accompanied by an increase in fracture energy. The observed increase is explained as a result of microcrack nucleation at intersection slip bands.

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Document Details

Document Type
Technical Report
Publication Date
May 14, 1975
Accession Number
ADA011688

Entities

People

  • C. Norman Ahlquist
  • Rishi Raj

Organizations

  • University of Colorado Boulder

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Adhesives
  • Boundaries
  • Ceramic Materials
  • Chemistry
  • Crystal Structure
  • Crystals
  • Grain Boundaries
  • High Temperature
  • Impurities
  • Materials
  • Materials Science
  • Measurement
  • Mechanical Engineering
  • Mechanical Properties
  • Metallurgy
  • Viscosity
  • Yield Strength

Readers

  • Materials Science (Mechanical Engineering).
  • Materials Science and Engineering.
  • Thin Film Deposition Science.