Development of High Pressure Liquid Chromatographic Techniques.

Abstract

Development of high pressure liquid chromatography detectors is discussed. Preliminary evaluation of a beta-induced luminescence detector employing a tritium source and operated in a luminescence quenching mode is presented. An ultrasonic velocity detector is described, along with calibration data, complete construction details, and operating instructions. A solid-state electrode for silver ion detection using a Ag6I4WO4 pellet is described, and calibration data and interference studies are presented. Construction of a beta-induced luminescence detector to be operated in a direct luminescence mode is described. Data for the recovery and preliminary characterization of refractory organics from treated wastewater using an organics-carbon minifilter are presented. The carbon chloroform extract of the minisampler is analyzed using high pressure liquid chromatography, and column parameters providing maximum resolution of components are given in detail. (Author)

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Document Details

Document Type
Technical Report
Publication Date
Oct 01, 1976
Accession Number
ADA039644

Entities

People

  • Edward A. Walters
  • James R. Matthews
  • Roy D. Caton Jr.

Organizations

  • University of New Mexico

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Energy and Power Technologies
  • Human Systems
  • Sensors

DTIC Thesaurus Topics

  • Alcohols
  • Chemical Synthesis
  • Chemistry
  • Detectors
  • Drinking Water
  • High Pressure
  • Ion Selective Electrodes
  • Ions
  • Liquid Chromatography
  • Literature Surveys
  • Materials
  • Measurement
  • New Mexico
  • Nitrogen Compounds
  • Organic Compounds
  • Solvent Extraction
  • Transducers

Readers

  • Analytical Chemistry
  • Fluid Dynamics.
  • Materials Science and Engineering.