Composition of Vapors Evolved from Military TNT as Influenced by Temperature, Solid Composition, Age, and Source

Abstract

A number of domestic and foreign military TNT samples were analyzed by a gas chromatographic headspace technique. The method allowed the determination of the vapor pressure of TNT and the partial pressures of several associated impurities over a 2 to 32 C temperature range. A major volatile impurity in all U.S. military TNT samples was 2-4-dinitrotoluene, which had a partial pressure 1 to 2 orders of magnitude higher than the vapor pressure of TNT. The experimental data followed a Clausius-Clapeyron temperature dependence for the vapor pressure of TNT, and the partial pressure of DNT was related to its concentration in the solid by a Henry' constant. Age and source of the TNT were found to have little or no influence on these relationships. The reasons for finding a relatively high DNT partial pressure are discussed, as is its implication for TNT detection by trace gas methods. (Author)

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1977
Accession Number
ADA040632

Entities

People

  • D. C. Leggett
  • R. P. Murrmann
  • T. F. Jenkins

Organizations

  • Cold Regions Research and Engineering Laboratory

Tags

Communities of Interest

  • Counter IED
  • Sensors

DTIC Thesaurus Topics

  • Chemistry
  • Chromatography
  • Detection
  • Detectors
  • Equations
  • Explosives
  • Gas Chromatography
  • Heat Energy
  • Materials
  • Measurement
  • Partial Pressure
  • Physical Chemistry
  • Solid Phases
  • Sublimation
  • Tnt
  • United States
  • Vapor Pressure

Readers

  • Analytical Chemistry
  • Combustion science or combustion engineering.
  • Naval Personnel Management