Adhesive Bonded Steel: Bond Durability as Related to Selected Surface Treatments

Abstract

High-strength 4340 carbon steel single lap-shear coupons were treated with four selected surface preparations: (1) wire brush, (2) sodium metasilicate/ Triton X-200 solution, (3) phosphoric acid/ethanol solution, and (4) potassium iodide/phosphoric acid (iodophosphate) solution. Bonded joints were made with all four surface preparations using 3M's EC 2214 epoxy and B. F. Goodrich's TAME 200 acrylic adhesive. The joints were subjected to lap shear strength-control testing at 23 C and 60 C, then to hot water soak at 60 C for 100, 500, and 1,000 hours followed by testing at 60 C and stressed durability at 60 C and 95% RH until failure. Results indicate only slight differences in control test results for the different surface treatments using EC 2214, but very large differences using TAME 200. Durability of joints using both adhesives clearly favors the iodophospate and phosphoric acid/ethanol treatments.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1977
Accession Number
ADA053944

Entities

People

  • A. T. Devine

Organizations

  • United States Army Armament Research, Development and Engineering Center

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Weapons Technologies

DTIC Thesaurus Topics

  • Adhesive Bonding
  • Adhesives
  • Aircrafts
  • Bonded Joints
  • Carbon Steels
  • Engineering
  • Failure Mode And Effect Analysis
  • Hot Water
  • Materials
  • Materials Laboratories
  • Mechanics
  • Munitions
  • Phosphoric Acids
  • Shear Strength
  • Shear Tests
  • Surface Finishing
  • Weapons

Readers

  • Materials Science and Engineering.
  • Surface Coatings Technology.