Degradable Binders for Ordnance Disposal

Abstract

The objectives of the current program are to prepare one or more candidate plastic bonded explosives (PBX) that will undergo controlled, thermal degradation to a processable material to provide the Navy with a degradable PBX for interim qualification. Under previous contracts, difunctional (OH) azo compounds incorporated into polyurethane binders provided a degradable PBX loaded with HMX. Under phase I of the current program we prepared a difunctional azo compound (the degradable binder unit) that can be used for RDX-loaded PBXs. In Phase II, we have formulated and tested PBXs containing optimum degradable units developed in Phase I. A thermally sensitive binder system has been developed for use in plastic bonded explosive (PBX) containing RDX filler. The thermally sensitive component in the formulations is the azo compound 1, 1- bis(3-hydroxypropyl) 1, 1, 1', 1'-tetraisobutyl azomethane (BPTA). This structure was selected based on its decomposition kinetics and ease of preparation. Because the compound is a primary diol, it is readily incorporated into crosslinked polyurethane binder formulations. The kinetic data indicate the binder has long-term stability with little change of physical properties at ambient conditions. However, when heated at 140C (for approximately 1 hr), the binder degrades from a resilient insoluble material to a viscous fluid that is readily soluble.

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Document Details

Document Type
Technical Report
Publication Date
Jun 16, 1978
Accession Number
ADA067791

Entities

People

  • Dale G. Hendry
  • Donald L. Ross
  • Gerald E. Manser
  • Richard A. Kenley

Organizations

  • SRI International

Tags

Communities of Interest

  • Engineered Resilient Systems
  • Weapons Technologies

DTIC Thesaurus Topics

  • Alkanes
  • Alkenes
  • Azo Compounds
  • Chemical Properties
  • Chemical Synthesis
  • Chemistry
  • Chlorides
  • Explosives
  • Gel Permeation Chromatography
  • Materials
  • Materials Laboratories
  • Materials Science
  • Molecular Weight
  • Organic Chemistry
  • Physical Properties
  • Plastic Bonded Explosives
  • Polymers

Fields of Study

  • Materials science

Readers

  • Agricultural Chemistry/Soil Science
  • Organic Chemistry
  • Polymer Science and Engineering.