Effect of Retained Austenite on Hydrogen Embrittlement of Steels.

Abstract

Ultrahigh strength steel alloys heat treated to 200,000 psi yield strength levels are notoriously sensitive to hydrogen induced delayed failure. In this program the effects of microstructure, especially that of retained austenite, on hydrogen induced (a) threshold stress intensity level, (b) crack growth rate, and (c) fatigue crack growth rate have been investigated. Microstructural variables investigated included prior austenite grain size, twinning, carbides, retained austenite, and indirectly, segregation. Emphasis in this study has been placed on the contribution of and stability of retained austenite. Optical, scanning electron microscopy, and transmission electron microscopy have been employed to establish microstructural details. Compact tension and bolt loaded fracture toughness specimens were used throughout the program. Precision hydrogen measurement were carried out by the Boeing Company. It was necessary to measure the hydrogen content for each sample, since it was not possible to introduce consistent hydrogen levels by cathodically charging. The influence of retained austenite is limited by its instability at the crack tip, where it has been shown to transform due to the intense stresses and strains in the plastic zone. Acoustic emission analysis was employed to detect and study the microscopic nature of crack growth as well as to establish a threshold stress intensity level. Test results showed that retained austenite, grain size, and probable segregation each contribute towards altering the hydrogen induced delayed failure characteristics. (Author)

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Document Details

Document Type
Technical Report
Publication Date
Nov 14, 1979
Accession Number
ADA078988

Entities

People

  • W. E. Wood

Tags

Communities of Interest

  • Air Platforms
  • Counter IED
  • Human Systems
  • Space

DTIC Thesaurus Topics

  • Acoustic Emissions
  • Alloys
  • Amplitude
  • Crack Tips
  • Electron Microscopy
  • Electrons
  • Emission
  • Grain Size
  • Heat Treatment
  • Hydrogen Embrittlement
  • Low Alloy Steels
  • Materials
  • Measurement
  • Microscopes
  • Microscopy
  • Resistance
  • Transmission Electron Microscopy

Fields of Study

  • Materials science

Readers

  • Materials Science (Mechanical Engineering).
  • Metallurgy

Technology Areas

  • Microelectronics