Zirconium Powder Characterization and Process Improvement for Thermal Batteries

Abstract

The inhouse program has resulted in a survey and characterization of existing production raw materials and product Zr metal powder as a heat source in the AF Maverick thermal battery. The variables most likely causing inconsistency and ignition sensitivity of zirconium metal powders are identified. The criteria for design and safety requirements for a laboratory scale zirconium-reduction-leach facility were established. The reduction and leach-wash cycle parameters were optimized to produce consistent quality fine particle 1-2-micrometer zirconium powder. The reduction scale up (400 grams per batch) was achieved in order to produce sufficient quantities of Zr metal powder for performance tests and to evaluate variables. The technology was transferred to the industry for production of 50 pounds/batch Zr metal was accomplished.

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Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1979
Accession Number
ADA080344

Entities

People

  • K. S. Mazdiyasni
  • Robert F. Geisendorfer

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics
  • Ground and Sea Platforms
  • Human Systems
  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force
  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemistry
  • Combustion
  • Controlled Atmospheres
  • Electron Microscopes
  • Electron Microscopy
  • Exothermic Reactions
  • Manufacturing
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Measurement
  • Pressure Measurement
  • Quality Control

Readers

  • Rocket Propulsion.
  • Software Engineering.
  • Surface Engineering/Surface Coating Technology.