Studies Relating to the Synthesis of Monomethylhydrazine by Chloramination and Problem Relating to the Protection of the Environment from the Vapors of 1, 1-Dimethylhydrazine, Monomethylhydrazine and Hydrazine

Abstract

The synthesis of monomethylhydrazine was successfully achieved by reacting solutions of hydroxylamine-O-sulfonic acid with methylamine in diglyme. The synthesis of 1,1-dimethylhydrazine was carried out in a similar manner with dimethylhydrazine. A mechanism for the formation of formaldehyde dimethylhydrazone by the reaction of dimethylamine and chloramine was proposed. A study was conducted on the oxidation of monomethylhydrazine and 1,1- dimethylhydrazine by oxygen.

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Document Details

Document Type
Technical Report
Publication Date
Sep 30, 1981
Accession Number
ADA108369

Entities

People

  • Harry H. Sisler
  • Milap A. Mathur

Organizations

  • University of Florida

Tags

Communities of Interest

  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Air Force
  • Amines
  • Chemical Synthesis
  • Chemistry
  • Chromatographic Analysis
  • Dimethylhydrazines
  • Environment
  • Formaldehyde
  • Hydrazines
  • Magnetic Resonance
  • Methylamine
  • Nuclear Magnetic Resonance
  • Organic Chemistry
  • Oxidation
  • Scientific Research
  • Sulfonic Acids

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry
  • Underwater engineering and Marine Technology.