The Effect of Anhydrous Ammonia on the Crystalline State Deformation of Nylons 6 and 6,6.

Abstract

The aliphatic polyamides Nylon-6 and -6,6 have been cold drawn using the new concept of reversible plasticization NH3. Two aspects were investigated: The effect of NH3 plasticization on the stress-strain behavior of nylon 6,6 and the extent of NH3 absorption studied by x-ray analysis and reported for the structurally simpler nylon 6. X-ray analysis shows that ammonia is absorbed preferentially by the amorphous phase and that the plasticization has a significant effect on the mode of crystal unit cell orientation, the small angle void scattering and the interplanar spacings between sheets of hydrogen bonded chains. The effect of plasticization was documented by the lower yield stress, the higher draw ratio (8x) and tensile modulus (10 GPa) not attainable with unplasticized specimens.

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Document Details

Document Type
Technical Report
Publication Date
Sep 14, 1981
Accession Number
ADA109582

Entities

People

  • Anagnostis E. Zachariades
  • Roger S. Porter
  • Tetsuo Kanamoto

Organizations

  • University of Massachusetts Amherst

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DTIC Thesaurus Topics

  • Chemical Engineering
  • Chemistry
  • Crystal Structure
  • Crystals
  • Diffraction
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  • Engineering
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  • Materials Science
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  • Military Research
  • Scattering
  • Strain Hardening
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  • Materials Science and Engineering.
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  • Polymer Science and Engineering.

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